Synthesis and Characterization of TosylHydrazone Complexes Derived from TosylHydrazone
Fernandesanil Juje1, H.V. Jayaprakash2
1Mr. Fernandesanil Juje, Department of Chemistry, Sri Siddhartha Institute of Technology, Tumkur-Kunigal Road, Saraswathipuram, Tumakuru (Karnataka), India.
2Dr. H. V. Jayaprakash, Department of Chemistry, Sri Siddhartha Institute of Technology, Tumkur-Kunigal Road, Saraswathipuram, Tumakuru (Karnataka), India.
Manuscript received on 13 October 2019 | Revised Manuscript received on 22 October 2019 | Manuscript Published on 02 November 2019 | PP: 989-992 | Volume-8 Issue-2S11 September 2019 | Retrieval Number: B11650982S1119/2019©BEIESP | DOI: 10.35940/ijrte.B1165.0982S1119
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© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: A new Schiff base ligand and complexes have been synthesized from tosylhydrazone 1,10phenonthroline and metal chloride salt of Ba(II), and Zinc(II) in acetonitrile medium. Several methods were used in particular; CHNS analysis, 1H NMR, IR, UV-Vis, Molar conductance, Magnetic moment and mass spectra. On the basis of elemental analysis and spectral examination, five corresponding geometries were given to these two complexes. Based on these these results, it is observed that this ligand acts as a bidentate and coordinates through oxygen and nitrogen atoms of the ligand. And 1,10phenonthroline binds through two symmetrical nitrogen atoms. Complexes are non-hygroscopic and photo stable solids at room temperature.
Keywords: Ligand, Metal Complex, Photo Stable., Schiff Base, Spectral Studies.
Scope of the Article: Network Traffic Characterization and Measurements