Ultrasound Synthesis and Antimicrobial Screening of Metal Complexes of 1– (5 – Chloro – 2– Hydroxyphenyl) – 3 – (2, 4 – Dichlorophenyl) Propane – 1, 3 – Dione
D.D. Suryawanshi1, S.T. Gaikwad2, A.D. Suryawanshi3, A.S. Rajbhoj4
1D.D. Suryawanshi, Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (Maharashtra), India.
2S.T. Gaikwad, Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (Maharashtra), India.
3A.D. Suryawanshi, Department of Physics B.J. College, Pune (Maharashtra), India.
4A.S.Rajbhoj, Department of Chemistry, Dr.Babasaheb Ambedkar Marathwada University, Aurangabad M.S., India.
Manuscript received on 21 July 2013 | Revised Manuscript received on 28 July 2013 | Manuscript published on 30 July 2013 | PP: 59-61 | Volume-2 Issue-3, July 2013 | Retrieval Number: C0708072313/2013©BEIESP
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© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: 1-(5-chloro-2-hydroxyphenyl)-3-(2,4 dichlorophenyl) propane-1,3-dione and its metal complexes Cu(II), Ni(II), Co(II), Cr(III) and Fe(III) have been synthesized by ultrasound irradiation method. The diketone is offered by employing Baker Venkatraman rearrangement. The synthesized compounds were confirmed by the spectroscopic analysis such as IR, 1H-NMR, 13C-NMR, mass, elemental analysis, magnetic susceptibility and evaluated for antibacterial screening.
Keywords: β-Diketone, Baker-Venkatraman Rearrangement, Metal Complexes, Magnetic Susceptibility, Antimicrobial Screening, Ultrasound Irradiation.
Scope of the Article: Design and Synthesis